The reflection of X-rays by crystals

Abstract In a discussion of the Laue photographs it has been shown that they may conveniently be interpreted as due to the reflection of X-rays in such planes within the crystal as are rich in atoms. This leads at once to the attempt to use cleavage planes as mirrors, and it has been found that mica gives a reflected pencil from its cleavage plane strong enough to make a visible impression on a photographic plate in a few minutes’ exposure. It has also been observed that the reflected pencil can be detected by the ionisation method. For the purpose of examining more closely the reflection of X-rays in this manner we have used an apparatus resembling a spectrometer in form, an ionisation chamber taking the place of the telescope. The collimator is replaced by a lead block pierced by a hole which can be stopped down to slits of various widths. The revolving table in the centre carries the crystal. The ionisation chamber is tubular, 15 cm. long and 5 cm. in diameter. It can be rotated about the axis of the instrument, to which its own axis is perpendicular. It is filled with sulphur dioxide in order to increase the ionisation current: both air and methyl iodide have also been used occasionally to make sure that no special characteristics of the gas in the chamber affect the interpretation of the results. The ionisation current is measured directly. A balance method has not been used as we have not found it possible to deflect a suitable portion of the primary rays into a balance chamber.