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The impending Euro 7 regulation will impose strict limits on brake particulate matter (PM) emissions from new light-duty vehicles, driving manufacturers to explore alternative rotor materials and/or surface treatments. This paper evaluates the friction and wear emission performance of both a laser-clad grey cast iron (GCI) rotor surface and a plasma electrolytic oxidation (PEO) treated aluminium surface compared to that of an uncoated GCI. Tests were conducted on a small-scale tribometer rig, which was specially adapted to measure airborne emissions while emulating the standard Worldwide harmonised Light vehicle Test Procedure (WLTP). The laser-clad coating was applied via extreme high-speed laser cladding to form an initial 430 L stainless steel layer, followed by a topcoat of 80/20 vol% 430L steel/TiC, both layers being c.100 micron thick. The PEO treatment applies a c.50 micron alumina coating to both a wrought and cast alloy, the latter being more suitable for the manufacture of full-size vented brake rotors. Results show that all rotor materials achieved a satisfactory coefficient of friction (CoF) against suitable low-metallic pad material, although the CoF for the wrought PEO-Al alloy was significantly higher at c.0.65 compared with c.0.50 for the other materials. The gravimetric wear of all the coated rotor surfaces after 8 WLTP cycles was almost undetectable, and pad wear was also significantly reduced. This improved wear resistance led to significant reductions in PM emissions, with the PM10 levels of the uncoated GCI reduced by around 75% for the laser-clad GCI and PEO wrought Al alloy, and by about 60% for the PEO cast Al alloy. When extrapolated to a full-sized passenger vehicle, the results indicated that both the laser-clad GCI and PEO-treated surfaces have the potential to meet the current Euro 7 emissions targets.