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The treatment of spent drilling fluids generated during the drilling of technological wells for uranium production represents an important engineering and environmental challenge associated with high energy consumption, significant waste generation, and the need for rational water use under arid regional conditions. Conventional phase separation methods based on gravitational settling and chemical–mechanical treatment are characterized by limited process controllability, long processing times, and increased consumption of reagents and energy. This study proposes an energy-efficient and reliable hydrodynamic technology for the treatment of spent drilling fluids based on the formation of controlled turbulent structures without the use of mechanical drives. The research object comprised spent drilling fluids (SDFs) generated during the drilling of technological wells for uranium production in the southern regions of the Republic of Kazakhstan and the Kyzylorda region. Experimental investigations were carried out using a laboratory–pilot hydrodynamic disperser with variations in velocity gradient, treatment time, flocculant dosage, and suspension flow rate. A mathematical model linking hydrodynamic process parameters with phase separation kinetics and energy characteristics was developed. Model calibration by weighted nonlinear least squares yielded a stable parameter set with 95% confidence intervals, and model validation demonstrated good agreement between calculated and experimental data (MAPE 8.4%; maximum relative error 11.8%). It was established that the use of a hydrodynamic disperser provides separation efficiency of up to 90–95% under optimal operating conditions while reducing specific energy consumption and maintaining stable repeated-cycle performance within the investigated operating window. Experimental results confirm that implementation of the hydrodynamic technology enables a reduction in sludge volume by 40–60%, recovery of up to 60–80% of process water, and a significant decrease in waste requiring transportation and disposal. The obtained results demonstrate the high environmental and resource-saving efficiency of the proposed technology and its suitability for scaling and industrial implementation at facilities drilling technological wells for uranium production. The developed hydrodynamic approach can be considered an effective engineering platform for creating energy-efficient and sustainable systems for drilling fluid treatment in regions with limited water resources and remote industrial infrastructure.